Merging all three volumes of the successful series "Spectroscopic Techniques: An Interactive Course" on NMR, this book serves as a practical approach and teaching tool for students and scientists applying NMR spectroscopy. By using the BRUKER software on the enclosed interactive CD-ROM, readers learn quickly and effectively how to operate a NMR spectrometer without wasting valuable spectrometer time. Thus, the beginner is not only guided from acquiring data to extracting spectroscopic details from an experimental data set, but is also confronted with a large variety of typical experiments. At the same time, trained users are introduced to more advanced experiments, such as 2D and 3D NMR spectroscopy, while the experienced NMR spectroscopist will discover ways to use the software for advanced 1D spectra simulation and iteration, including dynamic NMR. A cost-effective teaching tool, offering learning by doing and backed by hints, exercises and problems relating to data acquisition, processing and analysis.
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For beginners and experts: This practical guide includes interactive software and is an invaluable training tool for all NMR users! It covers not only a variety of NMR experiments, but also hints, exercises and problems relating to data acquisition, processing and analysis.
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INTRODUCTION Setup and Organization of TOPSPIN Components of TOPSPIN ACQUISITION STRATEGIES Building Blocks of an NMR Experiment Basic Acquisition Principles Magnetization Transfer Filtering and Selecting Experiments for Low-molecular Weight Samples One-dimensional Experiments Homonuclear Experiments Heteronuclear Experiments Accelerated Acquisition Experiments for Large-molecular Weight Samples Experiments for Medium-sized Samples Experiments using Labeled Samples Experiments to Overcome Fast Relaxation PROCESSING STRATEGIES Basic Processing and Plotting of Spectra Advanced Processing of One-dimensional Spectra Processing of Multidimensional Spectra Processing of Non-routinely Collected Data SPECTRA ANALYSIS General Characteristics of Spin Systems Structure and Spin System Parameters Time-dependent Phenomena REAL DATA COLLECTION AND ANALYSIS Odds and Sods of Real NMR Experiments Enhancement of Collected Data Tools for Automation Maximum Profits of a Collected Data Set
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Produktdetaljer

ISBN
9783527328710
Publisert
2011-07-20
Utgiver
Vendor
Blackwell Verlag GmbH
Aldersnivå
06, P
Språk
Product language
Engelsk
Format
Product format
Innbundet
Antall sider
450

Biographical note

Christian Schorn is NMR manager of the SP INTERVET Innovation GmbH in Schwabenheim, Germany. He studied chemistry at the University of Cologne and made his diploma thesis in chemical engineering in the central research department of the Bayer AG, Leverkusen. In 1997 he completed his PhD thesis on structural investigation using 19F NMR spectroscopy at the University of Cologne. For a post-doctoral stay he went to the University of Bern, Switzerland, where he worked on pulse program development and structural characterization in the NMR service laboratory of Peter Bigler. During his post-doctoral fellowship at the ETH Zurich, Switzerland, he worked with Nobel Prize winner Kurt Wuthrich on mammalian prion protein structures. From 2005 until 2007 he was Principal Investigator for GlaxoSmithKline R&D Limited, Tonbridge, UK. Christian Schorn has published with Wiley-VCH two editions of the volume "NMR-Spectroscopy: Data Acquisition" of the successful series "Spectroscopic Techniques: An Interactive Course".