Taking an organic chemistry laboratory course? You need a laboratory textbook you can trust! This proven book gives you what you need to conduct a variety of interesting microscale experiments with safety and ease -- while you develop an understanding of the special techniques these types of experiments require.
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Experiment 1. Introduction to Microscale Laboratory.
Experiment 2. Solubility.
Experiment 3. Crystallization.
Experiment 4. Extraction.
Experiment 5. A Separation and Purification Scheme.
Experiment 6. Chromatography.
Experiment 7. Infrared Spectroscopy and Boiling Point Determination.
Experiment 8. Simple and Fractional Distillation.
Essay: Aspirin.
Experiment 9. Acetylsalicylic Acid.
Essay: Analgesics.
Experiment 10. Isolation of the Active Ingredient in an Analgesic Drug.
Experiment 11, Acetaminophen.
Essay: Identification of Drugs.
Experiment 12. TLC Analysis of Analgesic Drugs.
Essay: Caffeine.
Experiment 13. Isolation of Caffeine from Tea or Coffee.
Essay: Esters -- Flavors and Fragrances.
Experiment 14. Isopentyl Acetate (Banana Oil).
Essay: Terpenes and Phenylpropanoids.
Experiment 15. Essential Oils: Extraction of Oil of Cloves by Steam Distillation.
Essay: Stereochemical Theory of Odor.
Experiment 16. Spearmint and Caraway Oil: (+)- and (-)-Carvones.
Essay: The Chemistry of Vision.
Experiment 17. Isolation of Chlorophyll and Carotenoid Pigments from Spinach.
Essay: Ethanol and Fermentation Chemistry.
Experiment 18. Ethanol from Sucrose.
Essay Molecular Modeling and Molecular Mechanics.
Experiment 19. An Introduction to Molecular Modeling.
Essay: Computational Chemistry -- Ab Initio and Semiempirical Methods.
Experiment 20. Computational Chemistry.
Experiment 21. Reactivities of Some Alkyl Halides.
Experiment 22. Nucleophilic Substitution Reactions: Competing Nucleophiles.
Experiment 23. Synthesis of n-Butyl Bromide and t-Pentyl Chloride.
Experiment 24. 4-Methylcyclohexene.
Essay: Fats and Oils.
Experiment 25. Methyl Stearate from Methyl Oleate.
Essay: Soap.
Experiment 26. Preparation of Soap.
Essay: Petroleum and Fossil Fuels.
Experiment 27. Gas Chromatographic Analysis of Gasolines.
Essay: Biofuels.
Experiment 28. Biodiesel.
Essay: Green Chemistry.
Experiment 29. Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination.
Experiment 30. Nitration of Aromatic Compounds Using a Recyclable Catalyst.
Experiment 31. Reduction of Ketones Using Carrots as Biological Reducing Agents.
Experiment 32. Resolution of Phenylethylamine and Determination of Optical Purity.
Experiment 33. An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol.
Experiment 34. Multi-Step Reaction Sequences: The Conversion of Benzaldehydeto Benzilic Acid.
Experiment 35. Triphenylmethanol and Benzoic Acid.
Experiment 36. Aqueous-based Organozinc Reactions.
Experiment 37. Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst.
Experiment 38. Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butanediol to Prepare a Natural Product.
Experiment 39. The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones).
Experiment 40. A Green Enantioselective Aldol Condensation Reaction.
Experiment 41. Preparation of an Unsaturated Ketone via Michael and Aldol Condensation Reactions.
Experiment 42. Preparation of Triphenylpyridine.
Experiment 43. The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-Butadiene.
Experiment 44. Relative Reactivities of Several Aromatic Compounds.
Experiment 45. Nitration of Methyl Benzoate.
Essay: Synthetic Dyes.
Experiment 46. Preparation of Methyl Orange.
Experiment 47. Preparation of Indigo.
Experiment 48. Formulation of a Paint and Art Project.
Essay: Local Anesthetics.
Experiment 49. Benzocaine.
Essay: Pheromones: Insect Attractants and Repellents.
Experiment 50. N,N-Diethyl-m-toluamide: The Insect Repellent "OFF".
Essay: Sulfa Drugs.
Experiment 51. Sulfa Drugs: Preparation of Sulfanilamide.
Essay: Polymers and Plastics.
Experiment 52. Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene.
Essay: Diels-Alder Reactions and Insecticides.
Experiment 53. The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride.
Experiment 54. The Diels-Alder Reaction with Anthracene-9-Methanol.
Experiment 55. Photoreduction of Benzophenone and Rear
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Produktdetaljer
ISBN
9781305968349
Publisert
2017-01-01
Utgave
6. utgave
Utgiver
Vendor
Brooks/Cole
Vekt
2177 gr
Høyde
40 mm
Bredde
220 mm
Dybde
276 mm
Aldersnivå
U, 05
Språk
Product language
Engelsk
Format
Product format
Innbundet
Antall sider
1056